Work up 1H NMR Spectrum in MNova (following along the NMR directions packet)
Chem240_DJS
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Work up 1H NMR Spectrum in MNova (following along the NMR directions packet)
219 просмотров · 1 год назад
Chem240_DJS
259 подписчиков
219 просмотров · 1 год назад
In the NMR worksheet lab, I provide a written NMR directions handout and spectra for 4-hydroxy-2-butanone. I then ask students to learn how to work up a 1H NMR spectrum by following along in the directions.
For students who struggle to learn from reading, or for those who want a quick refresher, I am providing this video.
Timestamps:
0:00 Overview
0:23 Showing the FID
0:39 MNova general navigation
0:59 Set a CDCl3 or TMS reference
2:14 How to perform Integration
2:48 Set a reference integral
3:54 Peak Picking tool
5:41 reporting chemical shifts of peaks
6:08 measuring J's with Crosshair tool
7:43 Wrap-up and Review of the Whole process.