How to Subtract Instrumental Broadening (βi) from XRD Data using OriginPro
SAYPhysics
0:00 / 0:00
How to Subtract Instrumental Broadening (βi) from XRD Data using OriginPro
13 060 просмотров · 5 л. назад
SAYPhysics
36,3 тыс. подписчиков
13 060 просмотров · 5 л. назад
Learn how to subtract instrumental broadening (βi) from XRD data using OriginPro.
This tutorial covers what instrumental broadening (βi) in XRD data is, what factors contribute to the instrumental broadening in XRD data, x-ray machine optics cause instrumental broadening in XRD data, and subtract instrumental broadening from XRD.
Origin and Excel Files:
https://drive.google.com/file/d/1Bqv1...
0:10 what is instrumental broadening (βi) in XRD data
2:25 what factors contribute to the instrumental broadening in XRD data
3:00 X-ray machine optics cause instrumental broadening in XRD data
6:20 how to subtract instrumental broadening from XRD
8:10 how instrumental broadening affect XRD parameters
All XRD Video Tutorials:
1. Baseline correction for XRD and FTIR data
• XRD & FTIR Baseline Correction in OriginPr...
2. How to smooth XRD graph
• How to Smooth XRD Graph in OriginPro
3. How to calculate the crystallite size from XRD data
• How to Calculate Crystallite Size from XRD...
4. How to put negative hkl indices in XRD graph
• How to Add Negative Hkl Indices to XRD Gra...
5. How to plot and match XRD data in WinXPow
• How to Plot XRD Data in OriginPro - from M...
6. How to calculate crystallinity index from XRD data
• How to Calculate Crystallinity Index from ...
7. How to calculate d-spacing (interplanar spacing) from XRD data
• How to Calculate D-spacing (Interplanar Sp...
8. How to calculate lattice constants from XRD data
• How to Calculate D-spacing (Interplanar Sp...
9. How to calculate microstrain from XRD data
• How to Calculate Microstrain from XRD Data...
10. How to calculate dislocation density from XRD data
• How to Calculate Dislocation Density from ...
11. How to subtract instrumental broadening (Kα1 and Kα2 overlap) from XRD data
• How to Subtract Instrumental Broadening (K...
12. How to subtract instrumental broadening (βi) from XRD data
• How to Subtract Instrumental Broadening (β...
13. Williamson-Hall Plot | W-H Plot | Crystallite Size | Microstrain | XRD data
• How to Subtract Instrumental Broadening (β...
14. Williamson-Hall Plot | W-H Plot | Crystallite Size | Microstrain | XRD data
• Williamson-Hall Plot | W-H Plot | Crystall...
15. Modified W-H Plots | UDM-USDM-UDEDM | Crystallite Size | Microstrain | Energy Density
• Modified W-H Plots | UDM-USDM-UDEDM | Crys...
References:
http://prism.mit.edu/xray
Article References
https://link.springer.com/article/10....
D. Balzar, N. Audebrand, M. Daymond, A. Fitch, A. Hewat, J.I. Langford, A. Le Bail, D. Louër, O. Masson, C.N. McCowan, N.C. Popa, P.W. Stephens, B. Toby, “Size-Strain Line-Broadening Analysis of the Ceria Round-Robin Sample”, Journal of Applied Crystallography 37 (2004) 911-924
•S Enzo, G Fagherazzi, A Benedetti, S Polizzi,
–“A Profile-Fitting Procedure for Analysis of Broadened X-ray Diffraction Peaks: I. Methodology,” J. Appl. Cryst. (1988) 21, 536-542.
–“A Profile-Fitting Procedure for Analysis of Broadened X-ray Diffraction Peaks. II. Application and Discussion of the Methodology” J. Appl. Cryst. (1988) 21, 543-549
•B Marinkovic, R de Avillez, A Saavedra, FCR Assunção, “A Comparison between the Warren-Averbach Method and Alternate Methods for X-Ray Diffraction Microstructure Analysis of Polycrystalline Specimens”, Materials Research 4 (2) 71-76, 2001.
•D Lou, N Audebrand, “Profile Fitting and Diffraction Line-Broadening Analysis,” Advances in X-ray Diffraction 41, 1997.
•A Leineweber, EJ Mittemeijer, “Anisotropic microstrain broadening due to compositional inhomogeneities and its parametrisation”, Z. Kristallogr. Suppl. 23 (2006) 117-122
•BR York, “New X-ray Diffraction Line Profile Function Based on Crystallite Size and Strain Distributions Determined from Mean Field Theory and Statistical Mechanics”, Advances in X-ray Diffraction 41, 1997.
#XRD #Crystallography #OriginPro